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Bulletin of the Chemical Society of Ethiopia

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Crystal structure of 2-(3,5-dimethoxyphenylamino)-3-chloronaphthalene-1,4-dione

N. Bayrak, M. Yıldız, H. Yıldırım, M. Sahin, A. F. Tuyun

Abstract


2-(3,5-Dimethoxyphenylamino)-3-chloronaphthalene-1,4-dione compound was prepared from the nucleophilic substitution reaction of 2,3-dichloro-1,4-naphthoquinone with 3,5-dimethoxyphenylamine at reflux temperature according to literature reported previously. Single-crystal X-ray diffraction analysis was carried out to confirm the structure of the title compound. The title compound, C18H14ClNO4, crystallizes in the triclinic space group P-1, a = 7.0016(6) Å, b = 7.7937(6) Å, c = 15.6218(11) Å, β = 97.238(4)°, V = 782.44(11) Å3, Z = 2, R1 = 0.0525, wR2 = 0.1329.

               

KEY WORDS: Naphthoquinones, Aminochloronaphthoquinone; X-Ray diffraction

 

Bull. Chem. Soc. Ethiop. 2018, 32(3), 603-608.

DOI: https://dx.doi.org/10.4314/bcse.v32i3.18




http://dx.doi.org/10.4314/bcse.v32i3.18
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