Synthesis, characterization and X-ray structure of an oxazine derivative

Iran Sheikhshoaie; Ferdinand Belaj; Ahmad Kamali

doi:10.4314/bcse.v24i2.54761

Iran Sheikhshoaie Department of Chemistry, Shahid-Bahonar Universirt of Kerman, Kerman, Iran
Ferdinand Belaj Institute of Chemistry, Karl-Franzens-University Graz, Schubertstr. 1, A-8010 Graz, Austria
Ahmad Kamali Department of Chemistry, Shahid-Bahonar Universirt of Kerman, Kerman, Iran

DOI: 10.4314/bcse.v24i2.54761

Keywords: 1, 2-Diphenylethanone, 1-Amino-2-propanol, Oxazine

Abstract

The 5,6-dihydro-6-methyl-2,3-diphenyl-2H-1,4-oxazine-2-ol compound (2) was prepared unambiguously by condensation of 1,2-diphenylethanone with 1-amino-2-propanol in the presence of glacial acetic acid. The product was characterized by FT-IR, ¹HNMR, UV-Vis spectroscopy and X-ray crystallography. Quantum chemical calculations are used to the proposed mechanism.

KEY WORDS: 1,2-Diphenylethanone, 1-Amino-2-propanol, Oxazine

Bull. Chem. Soc. Ethiop. 2010, 24(2), 283-287.

Synthesis, characterization and X-ray structure of an oxazine derivative

Abstract

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